GATE 2021 CE (CE1) – Question 38
A 50 mL wastewater sample is dried in a crucible. Empty crucible mass is 54.352 g; crucible plus dried sample is 55.129 g; after firing at 600°C for 1 h it is 54.783 g. Find total volatile solids concentration.
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Correct answer: (C) 6920 mg/L
Explanation
Volatile solids are the mass lost on ignition, not the whole dry residue. This loss is $55.129-54.783=0.346$ g=346 mg. Divide by 0.050 L to obtain **6920 mg/L (C)**. The empty crucible mass cancels in this difference.